International Journal of Science and Research (IJSR)

International Journal of Science and Research (IJSR)
Call for Papers | Fully Refereed | Open Access | Double Blind Peer Reviewed

ISSN: 2319-7064


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Student Project | Chemistry | India | Volume 12 Issue 8, August 2023 | Popularity: 5.3 / 10


     

Synthesis and Characterization of Some Metal Complexes Prepared from Schiff Base Ligand having Heterocyclic Unit

Sudhakar .G, Siddarth .H, Narsimlu T, Sudharani Nayak


Abstract: New series of co - ordination compounds of some transition metal ions [Zn (II), Ni (II), Cu (II) ] of synthesized ligand (4 - [2{5 - [4 - Nitrobenzylidene) - amino] - [1, 3, 4]thiadiazole - 2yl}phenylimino) - methyl] - phenol. These new prepared metal complexes and Schiff base ligand were characterised by elemental microanalysis (CHNSO), FTIR, UV - Vis, 1H - NMR, thermal analysis (TGA - DTA), magnetic susceptibility and molar conductance. Accordance to the obtained data all the prepared complexes were non - electrolytic. On the basis of the instrumental results, structures of metal complexes have been proposed. From the spectral data it is revealed that all prepared complexes exhibit 2: 1 (ligand: metal) ratio. Thermal data shows degradation of these complexes.


Keywords: Schiff base, synthesis, thermal analysis, 1, 3, 4 thidiazole, transition metal


Edition: Volume 12 Issue 8, August 2023


Pages: 1871 - 1874


DOI: https://www.doi.org/10.21275/SR23818122552



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Sudhakar .G, Siddarth .H, Narsimlu T, Sudharani Nayak, "Synthesis and Characterization of Some Metal Complexes Prepared from Schiff Base Ligand having Heterocyclic Unit", International Journal of Science and Research (IJSR), Volume 12 Issue 8, August 2023, pp. 1871-1874, https://www.ijsr.net/getabstract.php?paperid=SR23818122552, DOI: https://www.doi.org/10.21275/SR23818122552



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