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Research Paper | Physics Science | Iraq | Volume 3 Issue 10, October 2014 | Popularity: 6.6 / 10

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The Crystal Structure Analyses of Molecular Compound N-allyl-2, 6-di (ortho-chloro-phenyl)-4-methoxyphenyl pyridinium perchlorate using X-ray Diffraction Data

Mouayed M. Mahmoud, Saad N. Ibrahim

Abstract: The crystal structure of the N-allyl-2, 6-di (ortho-chloro-phenyl) -4-methoxyphenyl pyridinium perchlorate molecular compound was studied by X-ray diffraction. The structure analyses were carried out from diffraction data collected from single crystal of appropriate size. The lattice parameters are a=10.947Ao, b=10.996Ao, c=11.380Ao, =104.17o, =100.76o, =84.27o, monoclinic system, the space group is. The structure was solved by direct methods and refined by full matrix least-square calculation to a final discrepancy index R of 0, 048 for 2721 reflections. The co-ordinates, the thermal parameters, the bond lengths and angles of all atoms were measured.

Keywords: x-rays difraction, crystal structure

Edition: Volume 3 Issue 10, October 2014

Pages: 1507 - 1511

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